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Additional info for Techniques in Thermal Analysis: Hyphenated Techniques, Thermal Analysis of the Surface, and Fast Rate Analysis (ASTM special technical publication, 1466)

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36–43. [5] Morris, K. , "Structural Aspects of Hydrates and Solvates," Polymorphism in Pharmaceutical Solids, Marcel Dekker and H. G. , New York, 1999, pp. 125– 182. [6] Redman-Furey, N. L. and Collins, W. , "Thermoanalytical Characterization of Pharmaceutical Materials: Small Molecule Applications," American Pharmaceutical Review, Vol. 5, No. 1, 2002, pp. 102–107. Journal of ASTM International, July/August 2005, Vol. 2, No. org Adrienne S. Bigalow Kern,1 Wendy J. Collins,1 R. ,2 and Nancy L. 3 Use of a TG/DTA/Raman System to Monitor Dehydration and Phase Conversions ABSTRACT: Use of a TG/DTA/Raman system enabled real time collection of Raman spectra during the dehydration of Risedronate, the active pharmaceutical ingredient in the osteoporosis drug Actonel.

7] Morris, K. , "Structural Aspects of Hydrates and Solvates," Polymorphism in Pharmaceutical Solids, Marcel Dekker and H. G. , New York, 1999, pp. 125– 182. [8] Redman-Furey, N. , "Thermoanalytical Characterization of Pharmaceutical Materials: Small Molecule Applications," American Pharmaceutical Review, Vol. 5 No. 1, 2002, pp. 102–107. [9] Dicks, M. , Parsons, D. , and Redman-Furey, N. , "Concurrent Use of Thermal Analysis and X-Ray Powder Diffraction to Characterize Hydration States," Proceedings of the 30th North American Thermal Analysis Society Conference, B&K Publishing, K.

3 Use of a TG/DTA/Raman System to Monitor Dehydration and Phase Conversions ABSTRACT: Use of a TG/DTA/Raman system enabled real time collection of Raman spectra during the dehydration of Risedronate, the active pharmaceutical ingredient in the osteoporosis drug Actonel. Raman spectra collected during the dehydration of this material show a crystal lattice adjustment below the boiling point of water facilitating interpretation of the TG/DTA thermal profile. Raman spectra also revealed recrystallization processes subsequent to loss of lattice water that were not evident in the thermal analysis profile.

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