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Extra resources for Self-healing Materials
Adopted from  Self-Healing Polymers Based on Reversible Covalent Bonds 25 Fig. 13 Optical microscope images (left and middle) and corresponding SECM images (right) of the self-healing process: (a, d, g) Fractured surface before healing; (b, e, h) after 2 h, and (c, f, i) after 7 h of healing (Reproduced from . Copyright 2015 Wiley-VCH Verlag GmbH & Co. KgaA) In contrast to the classical DA systems, fulvene and electron-poor dienophiles feature a much higher reversibility, resulting in exchange even at room temperature.
For this purpose, the authors synthesized two similar copolymers on the basis of poly(4-vinylbenzyl chloride) (PCMS) with two different alkoxyamine units [2,2,6,6-tetramethylpiperidinyl-1oxy (TEMPO) and 1-(1-phenylethoxy)-2,2,6,6-tetramethylpiperidin (TEMPOEOPh)] as pendent groups (Fig. 25). After that, PCMS-TEMPO/PCMSTEMPO-EOPh blends were prepared to check the self-healing ability through radical crossover reactions. First, a solution of PCMS-TEMPO/PCMS-TEMPOEOPh was heated to 125 C for 20 min, resulting in the formation of a gel and, thus, proving the occurrence of cross-reactions.
For this purpose, the authors prepared two different poly(urea-urethanes) and mixed them in a certain ratio to obtain a material with good elastomeric properties. This material, which contained Self-Healing Polymers Based on Reversible Covalent Bonds 37 Fig. 20 Monomer structure of epoxy resins EPS25 and EPS70 and crosslinkers 4-SH and 3-SH; see text for details. Adopted from  Fig. 21 (a) Self-healing of a polymer, based on disulfide exchange reactions monitored by an optical microscope. (b) Example of macroscopic cohesion recovery (Reproduced from .
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