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31 [1976] 207/9). [23] Kennedy, J. D. (J. Chem. soc. Perkin Trans. 11 1977 242/8). ; Coucouvanis, D. (Inorg. Chem. 16 [1977] 1611/4). [25] Petridis, D. (Inorg. Chem. 17 [1978] 3719/21). [26] Knoth, W. H. (J. Am. Chem. soc. 101 [1979] 759/60). ; Engelhardt. ; Mägi. ; Larin. M. ; Pestunovich. V. A; Voronkov, M. G. (J. Organometal. Chem. 171 [1979] 301/8). [28] Zonnevijlle. ; Pope, M. T. (J. Am. Chem. soc. 101 [1979] 2731/2). ; Fischer, G. W. (Z. Anorg. Allgem. Chem. 463 [1980]123/31). , Ud. (Japan.

However, although the two terminal tin atoms are crystallographically equivalent owing to the disorder, they are not chemically equivalent. This is consistent with three types of tin atoms and three types of methyl protons indicated by the NMR spectra. Assuming that the solid state structure is the one present also in solution, the fluxional behavior implied by the NMR data can be explained bya ligand-exchange mechanism [35]. Gmelin Hendbook Organotin 17 References on p. 23 2' 20 Table 2 NMR Data of CH3Sn(OCH2CH2)3N [27].

19711073). ; Koola, J. (J. Organometal. Chem. 31 [1971] 59/66). ; Burger, K. (J. Organometal. Chem. 59 [1973] 199/206). ; Pönicke, K. (J. Organometal. Chem. 51 [1973] 197/201). Kennedy, J. ; McFarlane, W. (Rev. Silicon Germanium Tin Lead Chem. 1 [1974] 235/98). ; sharma, H. ; Carty, A. ; Walker, A (Inorg. Chem. 13 [1974] 1205/11). van den Berghe, E. ; van der Kelen, G. P. (J. Mol. struct. 20 [1974] 147/52). ; Miller, J. M. (J. Chem. soc. Dalton Trans. 1975393/5). Tzschach, A; Pönicke, K. (Z. Anorg.

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