By Krause W.
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Extra resources for Contrast Agents III
Sample text
Acp is water-soluble and reasonably stable. The reaction with [99Tc(OH2)3(CO)3]+ in phosphate buffer resulted in the formation of [99Tc(ACp)(CO)3] in 10–40% yield. The yield is not quantitative owing to the hydrolytic formation of [Tc4(m3-OH)4(CO)12], which is the competing side reaction to the formation of cytectrene. Since tetramerization does not occur in highly dilute solutions, the same reaction was carried out with 99mTc and re- 30 R. Alberto a b c Scheme 20 Fully aqueous preparation of a [Cp99mTc(CO)3] labelled biomolecule, enabled by the carbonyl group directly attached to the cyclopentadienyl-ring: a two-step approach, b direct one-step procedure and c observed by-product from carbonyl reduction by boranocarbonate sulted in quantitative formation of [99mTc(ACp)(CO)3] after 30 min at 95 °C.
79 . . . . . . . . . . . . . . . . . . . 80 References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Abstract This review presents a comprehensive overview of the most significant developments in the chemistry of technetium and rhenium complexes anchored by heterofunctionalized phosphines and by hard and soft scorpionates. The main goal is to provide the reader with chemical, radiochemical and biological knowledge which is expected to enhance the application of these types of compounds in the development of target-specific radiopharmaceuticals.
Most of the papers describe labelling chemistry with the fac-[99mTc(CO)3]+ moiety and a lower number of papers with Tc(III) complexes comprising one Tc–C bond to an isonitrile. Since the application of organometallic compounds in life science is recent, systematic studies are not available yet and the most important research results will be discussed in the following sections. 1 CNS Receptor Ligands A good overview of CNS receptor binding 99mTc-labelled complexes became available recently [88].
